ATTACHMENT C - CRITICAL REVIEW
This section reviews work accomplished toward meeting the objectives
ofNC-136 during the five-year period 1995-2000. The scope of the
scientific output is
indicated by the five-year list of peer-reviewed publications
from participating stations, found at the end of this review.
The Critical Review will emphasize work and
its impact, resulting from the cooperative efforts of the participating
scientists.
Major accomplishments The sharing of ideas, approaches, results
and critical reviews was the single most important accomplishment
of the project. Annual
meetings for the project presented a forum for collective discussion
involving the largest group of researchers in the U.S. interested
in advancing thermal processing
of foods. The format of annual meetings allowed detailed presentation
of collaborative and other research efforts to the entire group.
This provides a critical review
of the research on an ongoing basis. Critical and constructive
comments continue beyond the duration of presentation and often
lead to new and enhanced
collaborations. Members often commented that NC-136 is one of
the most important professional meetings that they attend.
Table Cl. Major accomplishments of NC-136, 1995-99
Number (multistation) | |
Journal articles, peer reviewed | 520 (17) |
Books and book chapters | 102 (7) |
Presentations | 320 (8) |
Theses and dissertations | 92 |
Patents | 15 |
USDA NRI grants | $1.75 million |
Other competitive grants | Over $16 million |
Impact
The project has contributed greatly to the development of food
thermal processes based on sound fundamental principles. Detailed
impact statements can be found
following accomplishments in each of the research topics described
under the three objectives. Collaborations of multiple stations
in several ad-hoc committees on
rheological properties of foods and their measurement techniques
have led to development of standard measurement procedures. Such
standard methods reduce
operator and instrument variability and provide more accurate
data for product and process design. NC-136 made such collaboration
possible. In phase transitions
in foods, collaboration has led to an IFT Basic Symposium as well
as an authoritative book on the subject, in addition to scientific
accomplishments. Thermal analysis
using the DSC was standardized by a six station-subcommittee so
that more accurate data can be obtained in the difficult measurement
process of glass transition.
An authoritative reference book on microwave processing of foods
is being published as a result of collaboration between stations.
Guidelines for aseptic processing
were developed in a workshop organized by several of the stations
by obtaining people from academia, industry and government. Development
of a new process of
microwave sterilization that ensures food safety while improving
product quality benefited significantly from collaboration between
NC-136 stations. Validation of
commercial sterilization to ensure food safety requires critical
kinetic parameters that were developed through collaborative studies
between stations. The sharing of
information and the cooperation fostered by NC 136 were directly
responsible in initiating and carrying out these important tasks
relative to food research.
Dissemination of information
Information generated in this project was made available to others
through the 320 presentations at national meetings and 354 publications
in widely-read scientific
journals, plus reference books, development of several short courses
and a website specifically developed for NC136. Two short courses,
one on aseptic
processing and one on the emerging processing technologies were
developed through collaboration of a number of stations. These
workshops were very well
attended by personnel from food processing and equipment industry,
government and academia. Two symposia were developed for Annual
IFT meetings that attract
the largest audience from food industry and academia. Impact to
education has also been very significant as the cutting edge research
in quality and safety of food
processing was included in graduate and undergraduate courses
taught at the participating stations.
Although the accomplishments of NC-136 have been impressive,
continued cooperative work in many areas is critical. Consumer
convenience and safety,
preference for healthier and tastier foods, and the use of new
food processing technologies mandate continued research. Our proposed
objectives for the next five
years are slightly modified to reflect this goal. The remaining
section is organized in terms of the three objectives of the completed
project with the accomplishments
and the continued needs for research discussed under each subtopic.
OBJECTIVE A:
To Identify and Quantify Important Physical and Biochemical
Properties of Thermally Processed Foods and Factors Affecting
These Properties
Al. Rheological Properties. Rheological (deformation and flow) properties of foods strongly influence food quality, safety and the design of processing and handling systems. Studies include rheology of fluid and semi- solid foods, development of improved measurement techniques, mathematical modeling of material behavior, and rheology for process design.
Al.l Improved Measurement Techniques. The Yield Stress
Subcommittee consisted of numerous stations (IA, MI, MO, NY-Geneva,
ND, OH, PA) over
several years of the project. During the course of this study,
each station developed the capabilities to measure the yield stress
of fluid and semi-solid foods using the
vane method. Identical products (applesauce, ketchup, and chocolate)
were tested by each station using carefully defined methodology.
The subcommittee met
every year to discuss previous results and plan subsequent trials.
Working within the infrastructure provided by NC-136, the group
was able to achieve the primary
objectives of the subcommittee: 1) to establish the controlled
rate vane method as a standard procedure for measuring yield stress,
and 2) to establish standard
terminology (static versus dynamic yield stress) to describe the
time- dependent nature of the phenomenon. The new procedure has
wide applications in the food
industry.
A Brookfield Viscometer equipped with a small sample adapter
(18 ml) and a flag impeller was used to evaluate the average shear
rates of mixing processes (Briggs
and Steffe, 1996). A shear rate value of 2.92 /rad is recommended
for routine work. Results were compared to those from a controlled
stress rheometer and
excellent agreement was found. This system provides a useful,
low cost, means of testing power law fluids. Mitschka's method*
to convert Brookfield instrument
readings into viscosity values was evaluated using disc-type spindles
(Briggs and Steffe, 1997), and found to be acceptable for many
fluid foods. Also, a vane tester
was designed and constructed to measure the yield stress of ice
cream at typical scooping temperatures of-12°C to -16°C
(Briggs et al., 1996). Yield stresses from
2.5 to 8.0 kPa were observed. This technique makes it possible
to objectively evaluate reduced fat ice cream formulations.
A direct-drive concentric cylinder viscometer in a pressure
chamber was used to study the flow behavior of a 11 °Brix
tomato puree over the temperature range : 76
to 120 °C, and the apparent viscosity versus temperature profiles
of a 4.0% waxy rice starch dispersion during continuous heating
from 30 to 110 °C (Rao et al.,
1999).
Future Needs: Rheological methods need to be developed for many foods including nonhomogeneous fluids and foams.
A1.2 Studies on Fluid and Semi-solid Foods Rheological
properties of fluid and semi-solid foods are being characterized
at the MI, NC, NY- Geneva, and WA
stations. They have dealt with understanding the role of composition
on the properties and measurement techniques. In a collaborative
study between the MI and
NY- Geneva stations, measurement of yield stress using the vane
method and the role of yield stress in suspending solid foods
were reviewed (Rao and Steffe,
1997). This helped develop "state-of- the-art" methodology
for other stations.
Rheology of wheat dough was studied in terms of the influence
of energy level, type of deformation (shear versus extensional)
and strain history on dough
development (Campos et al., 1997). Results indicate a strong correlation
between the degree of deformation and the development of protein
structure in wheat
dough. These results may lead to significant improvements in the
process and product development in the baking industry.
Various starches, proteins and their combinations were studied
to identify the effects of interaction between the components
and temperature on their rheology.
Rheological studies on cornstarch and waxy maize dispersions showed
that the consistency index of the dispersions increased exponentially
with mean granule
diameter (Okechukwu and Rao, 1995; 1996). Starch granules also
played an important role in the rheology of mixed wheat starch-gluten
pastes (Champenois et al.,
1998) and waxy maize starch dispersions (Chamberlain et al., 1999).
Such data are important for designing a number of thermal processes.
Dynamic rheological data revealed weak gel-like behavior of
both 10% corn starch and soy protein isolate (SP) dispersions;
the storage modulus of cornstarch
dispersion was higher than that of SP isolate. Plots of protein/starch
ratio vs. storage modulus revealed phase separation and inversion
(Chen et al., 1996; Liao et al.,
1996). In protein and starch gels (cowpea protein and 10% solids
cowpea starch), the modulus increased due to aging and starch
concentration. These results led to
important product improvements by increasing our understanding
of ingredient functionality.
The studies of Champenois et al. (1998) improved our understanding
of starch and gluten interactions in starch pastes. The addition
of gluten changed considerably
the viscoelastic properties of starch pastes. In starch dispersions,
the rheological unit was a starch granule. When gluten was present,
the rheological units were the
"cells" formed by gluten fibrils and filled by starch
granules. The internal lipids in flour played an important role
so that flour is not a simple blend of starch and gluten.
Results lead to improvements in the texture of bakery products.
Viscosity of a starch dispersion as a function of temperature
and shear rate during gelatinization are found in the temperature
range 60-95°C (Yang and Rao, 1998;
Lao et al., 1999). These data are needed, for example, in establishing
the safety of thermal sterilization of foods containing starch.
Electrorheology (ER) is the area of rheology that evaluates
changes in material flow properties during exposure to electric
fields. Applications of this technology in the
food industry may unleash new techniques for traditional processing,
and was studied for chocolate. The voltage altered the rheological
behavior of the fluid - voltage
polarized particles prompting structure formation in the fluid,
leading to a greater resistance to flow. In the absence of an
electric field, practically all fluids exhibit a
decrease in the apparent viscosity at higher temperatures. The
opposite response described here is typical of the unusual behavior
found in ER fluids (Daubert and
Steffe, 1996). A prediction equation was developed that allows
prediction of chocolate viscosity during exposure to electric
fields, and delivers a means of selecting
and controlling milk chocolate viscosity with voltage (Daubert
et al., 1998). Much work, however, still remains to harness this
technology in the form of food
processing applications. The chocolate industry may benefit from
this technology by externally controlling the flow properties
of milk chocolate, allowing the
development of new processes and products.
Future work: Due to the complex nature of foods, much more
work needs to be conducted in order to understand the role of
composition and their interactions on
the viscous and viscoelastic properties. As a first step, work
on food polymers should help our understanding of the role of
macro and microstructures, and
rheological elements on food rheology.
A1.3 Rheological Properties During Various Processes
Measurement of the rheological properties of fried product and
frying medium as an important aspect
of food frying research. One of the most important quality attributes
of a fried product is its crispness. Development of texture the
during frying process was studied
(Fan et al., 1997; Pinthus et al., 1998; Normen et al., 1998;
Rovedo et al., 1999). The influence of various components of starch
and post-frying moisture migration
on the texture and other mechanical properties of fried products
was studied. Force-deformation studies have been performed by
several researchers to predict
texture of fried products such as French fries and tortilla chips.
In general, a fried product becomes tougher as frying time increases
up to an optimum value after
which the product becomes brittle. Porosity and pore size distribution,
important for texture and oil absorption, were evaluated at the
TX station. Changes in oil
viscosity due to degradation and temperature changes during a
frying process, with major implications in the rate of heat, moisture
and oil transfer were also studied
at the CA and TX stations. Based partially on these studies, an
optical sensor for monitoring changes in oil quality has been
developed for use in industry.
Future Needs: Although considerable progress has been made
in the measurement and understanding of physical properties of
the oil and food product during
frying, there is still work needed to improve textural quality
and reduce oil absorption in frying. There is lack of data on
critical properties such as permeability of
porous food materials. A method to determine the surface tension,
between the oil and the product, needs to be developed so that
the effect of oil degradation and
surface interaction during the process can be better described.
A2. Phase Transitions in Foods During heating and cooling
of foods, there are many phase transitions that may change the
physical properties of the material.
These transitions are important in a wide range of food products,
including frozen foods, confectionery products, cereals, milk
powders, and many starch-based
foods. It is important to understand these phase transitions and
to be able to control them so the desired attributes are obtained
in the product. Many components of
foods undergo phase transitions (i.e., ice freezing, starch gelatinization,
glass transition, crystallization of sugars and lipids, etc.),
and research in this area by NC-136
members (led by NY-Geneva and WI) has led to publication of a
book on the topic of Phase/State Transitions in Foods.
Cooperative research headed by the OR, WI, and IA stations,
with contributions from 6 other stations (MN, MO, NE, NJ, ND,
OH) on a round robin differential
scanning calorimetry thermal analysis study to determine onset
and peak transition temperatures and enthalpy was completed (Kolbe
et al., 1998). The
reproducibility of these measures using three types of commercial
equipment for both starch gelatinization and tristearin melting
and crystallization was determined. he
transition temperatures and enthalpy values for starch were similar
among laboratories, as were the melting and crystallization temperatures
for tristearin. Enthalpy
values for tristearin were consistent among most laboratories,
but significant differences existed between DSC types. Based upon
the findings of the cooperative
study, instrument usage and laboratory conditions play a major
role in determining transition temperatures and enthalpy values.
Interdependent station activities may
prove useful for determining expected errors in other DSC measurements,
and the evaluation of new calibration materials. This research
will be continued with further
collaboration between the OH, WI, NE and IA stations. Additional
standardization of enthalpy measurements and the standardization
of the procedure to determine
the glass transition temperature of water in different food systems
will be investigated.
The effects of various operating parameters on the kinetics
of crystallization (sugars, lipids, and ice) have been measured
for different foods. For example, the
changes in ice crystals during storage and distribution of ice
cream were modeled based on previously determined kinetic parameters.
The effects of temperature and
extent of temperature fluctuations on recrystallization kinetics
were determined (Donhowe and Hartel, 1996) and then used to model
changes during normal shelf life
conditions (Ben-Yoseph and Hartel, 1999). These results clearly
show the beneficial effects of maintaining low temperatures during
the early stages of storage in the
process plant. Study on the effects of processing parameters on
crystallization of lipids showed that depending on process conditions,
foods with different mechanical
properties could be produced simply by altering the lipid crystalline
structure (Hen-era and Hartel, 1999a and b). By understanding
the relationships between
crystallization conditions and structural properties, we can control
the mechanical properties of lipid-based food products.
There is increasing evidence suggesting a unique relationship
between the glass transition temperature of a food and the rate
of quality change during the storage of
low moisture and frozen foods. Effects of glass transitions on
shelf life and quality in low moisture and frozen foods are being
investigated at MN, MO, NJ, and OH
stations.
Structure development rates in a gel, its melting temperature,
and enthalpy of melting were studied as a function of composition.
For example, high-methoxyl
pectin-Na alginate-fructose (65%) showed a stronger dependence
on Na alginate content than on sugar or pectin content (Rao and
Cooley, 1995). Physical gels
develop slowly and structure development rates provide quantitative
information. These data should be useful in scheduling gel-production.
While the enthalpy of
melting of sucrose gels was higher than those of plain gels, that
of sorbitol gels was lower, reflecting the important role of the
hydroxyl groups in the sugars (Fu and
Rao, 1999). Gel melting temperatures were also studied that should
be useful in selecting ingredients, such as pectins, and in developing
gels with a specific melting
temperature.
Several methods are currently available for measuring the glass
transition temperature of a food including DSC, DMA (Dynamic Mechanical
Analysis), and TMA
(Thermal and Mechanical Analysis), etc. The results often differ
from each other due to differences in the testing methods as well
as testing procedures such as
heating rate or frequency. Our DSC ad-hoc committee has started
to develop a protocol for measurement and analysis of the glass
transition temperature using
DSC. This protocol should reduce instrument and operator dependence
of the data and make it more consistent and reliable for design
of products and processes.
Future Work: Our understanding of phase transitions during
heating and cooling of foods is still severely lacking due to
the complexity of most foods. The
interactions between components in real foods make extrapolation
of results from pure, model systems very difficult. It is the
effects of these complex interactions
that will be the focus of most future work in this area. Most
of the glass transition temperatures reported in the literature
so far are limited to classical single-phase
food products. Data on multi-phase food products are needed for
the food industry to develop new and innovative food products.
A3. Colloidal and Interfacial Properties of Foods Colloidal
constituents affect and determine the behavior of many foods,
including milk, ice cream, butter,
mayonnaise, and cheese, all of which derive their characteristic
properties from the fact that they are colloids. As a result,
colloid and interface science provides a
microscopic framework for understanding and characterizing many
macroscopic food behaviors, including bulk rheological behavior,
and structural integrity of
emulsions and foams. For example, the adsorption, distribution
and/or interactions of proteins and surfactants at the liquid-liquid
interface determine the behavior of
all food emulsions and microemulsions. This, in turn, determines
such properties as shelf life and foam stability. An important
advantage of colloid and interface
science is that its fundamental principles can be used to study
materials that appear to be disparate. Therefore, lessons and
techniques from other fields of study can
be used to benefit food systems. This provides a powerful tool
that enables one to a gain molecular-level understanding of macroscopic
food behavior.
Work done at the MI Station so far has focused on the adsorption
and interactions of proteins at the oil-water interface. The recent
development of a total internal
reflection fluorescence microscopy technique has allowed for quantitative
molecular-level investigations of macromolecular adsorption and
interactions at liquid-liquid
interfaces. This apparatus, coupled with fluorescence photobleaching
recovery (FPR), has been used to qualitatively establish the relative
importance of bulk and
surface diffusion of representative proteins at the oil-water
interface. We have developed a procedure for calculating interfacial
protein concentrations on the basis of
fluorescent emission data, and studied the effect of extrinsic
fluorescent labels on the adsorption and diffusion of proteins.
Future Work: Work in the upcoming funding cycle will focus
on the interactions of various food proteins and commonly used
surfactants at the oil-water interface.
In particular we will investigate the competitive adsorption of
a-casein and b-casein (the two major milk proteins) in the presence
of surfactants such as the tweens.
We will seek collaboration with other stations on how the interfacial
adsorption/interactions of various food proteins and surfactants
affect the uptake and/or delivery
of selected nutrients and vitamins. This is a major undertaking
that should be of a great deal of interest to the food industry,
and will benefit from current collaborative
work with the OR station in which we are exploring the efficacy
of using proteins as drug delivery instruments.
A4. Electrical Properties of Foods
A4.1 Dielectric Properties of Foods for Microwave and Pulsed
Electric Field (PEF) Processing. For the food industry and
the consumer to benefit from the
convenience of microwave heating knowledge of dielectric properties
and how they change during processing are critical. Studies on
dielectric properties are being
conducted at the OH, PA and NY-Ithaca stations. Collaborative
work between OH and NY-Ithaca was presented in the 1997 Conference
on Food Engineering.
Dielectric properties of foods were measured in the range from
0 to 130 °C for the first time which is important for microwave
food sterilization processes. Phase
changes, such as starch gelatuzation and protein denaturation
during heating, changes the dielectric properties that have implication
in the sterilization process.
Changes in dielectric properties of cheese as a function of storage
time showed significant changes, of implication to microwave heating
of pizza and other cheese
containing products. Some of these studies are part of a larger
collaboration between the stations and other agencies (U.S. Army
Natick Laboratories) to determine
the dielectric properties at sterilization temperatures, and use
this information in better understanding microwave sterilization.
Microwave sterilization is being used in
Europe to produce high quality commercially available meals -
such technology can improve the quality of foods for our consumers
and soldiers in combat and make
it possible to export high value commodities.
Dielectric strength is the magnitude of electric field at which
the insulating properties breakdown and there is a discharge.
Systematic data on dielectric strength of
various food products are needed for design of ohmic heating and
pulsed electric field processing that can improve the quality
of processed food significantly.
Dielectric strength of various liquid foods with small size air
bubbles were determined (WA). Air bubbles break down in liquid
foods at an electric field of 22 to 25
kV/cm. De-aerated samples were able to withstand more than 80
kV/cm of electric field without breakdown. Pressurization of the
food increases the dielectric
strength of foods and makes it possible to allow the application
of PEF technology (OH) in some situations Without such critical
information, novel technology (such
as PEF) for improved food quality cannot be implemented.
Future work: Future needs are to measure the dielectric
properties at sterilization temperatures for a wide range of food
items, understand the changes in the food
that contribute to changes in dielectric properties and develop
accurate predictive models at these temperatures. Dielectric properties
of frozen and partially frozen
foods are needed. Such data will provide understanding of how
the dielectric property changes during the freezing/thawing process,
which is necessary for designing
products such as frozen microwaveable dinners.
A4.2 Electrical Conductivity of Foods for Ohmic and PEF
Processing Electrical conductivity information required for
the design of ohmic heaters for aseptic
processing has been measured and empirically modeled for various
model solutions and multiphase foods such as beef stew (OH and
NCFST stations). Electrical
conductivity has also been measured in the context of pulsed electric
field (PEF) processing (WA). In general, the electric conductivity
measured in a high voltage
pulse field is 10 to 20% higher than that measured with a DC type
electrical conductivity meter. This is attributed to electrolysis
during DC type measurements and
temperature increase of the sample under high voltage PEF measurements.
Electrical conductivity of liquid foods for a range of processing
temperatures have been
accomplished for low pulse field which are in good agreement with
high pulse field (OH). A database is being established for the
design of electro technology based
food processes (OH).
A5. Kinetics Collaborative work between FL and NC stations
has continued to evaluate the performance of two alternative techniques
for the determination of
kinetic parameters under dynamic temperature conditions (Moody,
1997). These kinetics provide the engineering parameters upon
which the design and validation
of commercial sterilization and pasteurization processes are based
in the food industry.
Bacterial and enzyme kinetics are needed for development of
new pasteurization processes. Kinetics of microbial load and trypsin
inhibitor in soymilk were studied
by the IA and ND stations. They demonstrated that times and temperatures
greater than those required for the pasteurization of cows milk
are required for soymilk.
Coagulation kinetics of soymilk to manufacture tofu were studied
to develop methods to monitor coagulation in the manufacture of
torn. The influences of processing
method, protein composition, soybean variety, and whole vs. flaked
soybeans on the yield and composition of torn were reported by
both stations (Moizuddin et al.,
1998; 1999). All of these studies have improved the thermal processing
of soybeans into soyfoods. Industries are currently utilizing
these findings to improve the
quality and safety of their products. Based upon these studies
a new reduced-fat tofu was introduced into the marketplace.
Kinetics of several microbiological changes were studied, with
implications to food safety. These included Salmonella dublin
exposed to pulsed electric field,
thermal destruction of E. coli 0157:H7 in a slaughterhouse operation,
Listeria monocyotgenes Scott A. in milk under conventional and
microwave heating, and
Fusarium mold growth during barley making. Kinetics of several
biochemical changes were studied, with applications to new product
and process development.
These included degradation of capsaicin or spice heat (Roche-Herrera
and Wilson, 1999), formations of pyrazines (aroma/flavor) during
Maillard reaction,
degradation of chlorophyll in pureed green peas, retention of
flavor during extrusion, and contribution of chlorination in cake-baking.
Future Work: Kinetic data is still needed for the improvement
and development of thermal and alternative processes. The influence
of the glass transition
temperature on these processes and products needs to be investigated
using reliable methods (DSC Ad-hoc Committee is looking into this).
This includes the
determination of kinetics associated with microbiological, enzymatic,
chemical, safety and quality changes. This data will be used by
multiple stations to design and
validate methods for the commercial processing of foods that are
safe and nutritious, with high consumer acceptance (sensory properties).
Multi-station collaboration
will continue in this area.
OBJECTIVE B:
To Identify And Describe Mechanisms For Heat, Mass, And Momentum
Transfer In Thermally Processes Foods And The Extent To Which
They
Are Affected And Governed By Parameters Covered By Objective A
Bl. Aseptic Processing of Fluid Foods and Particulates Aseptic
processing can provide much improved food quality and more efficient
industrial processing.
Aseptic processing has entered the mainstream as an industry practice
for fluids, but its application to particulates is currently limited.
Aseptic processing of
particulates has been widely investigated over the past fifteen
years. A NCFST-CAPPS (National Center for Food Safety and Technology
and Center for
Advanced Processing and Packaging Studies) workshop, co-sponsored
by several of the NC-136 participating stations and with participants
from several other
NC-136 institutions, has been termed "historic" in terms
of defining the safety considerations required (Damiano, 1997;
Degeronimo et al., 1997; Larkin, 1997;
Marcy, 1997; Sastry, 1997). Discussions during the workshop have
subsequently resulted in a successful process filing by Tetra
Pak. However, there has been no
major attempt by companies to file a process since that time.
Industry reluctance to file processes may be attributed in
part to caution, partly to the extensive filing requirements,
or a lack of significant quality advantages for the
technology if all the safety issues are addressed to the satisfaction
of the Food and Drug Administration. Consequently, it is still
necessary to improve the safety of
processes further while not sacrificing quality; i.e. a major
effort in optimization is necessary. In addition, the advent of
nonthermal process technologies has
introduced a new dimension of complexity to the task.
In the area of particulate-fluid flow, studies have ranged
from applied work on residence time distribution to a number of
fundamental studies aimed at modeling
solid-liquid flows (Liu and Zuritz, 1995; Hu, 1996; Lareo et al.,
1997; Unluturk et al., 1999). While these are useful in characterizing
average flow outcomes for
mixtures, the prediction of real food flows with large particle
loadings has remained elusive.
Estimation of solid-liquid heat transfer coefficient is in
the heart of developing aseptic processing of particulate foods.
Various measurement techniques have been
developed to determine realistic values of heat transfer coefficients
(Barigou et al., 1998) needed for development of microbiologically
safe processes. Alternative
methods of heating such as ohmic and radio frequency continue
to be investigated (Orangi et al., 1998; Sastry and Salengke,
1998).
Future Work: While fluid processing is now routine,
a major opportunity exists to reduce process requirements by applying
thermal and nonthermal processes
individually or in combination to produce high quality liquid
products. The kinetics of such processes are yet to be investigated,
although IFT is conducting a study for
FDA on the kinetics of alternate process technologies. Future
improvements in the technology will not only need to deal with
safety assurance, but also improve
product quality significantly, as with internal generation (ohmic,
radio frequency and microwave heating) and nonthermal processes.
Convective heat transfer
coefficient between solid particles and fluid show a wide variation
between laboratories, indicating the need to develop comparable
methodologies. Effects of various
processing parameters when using internal heat generation would
need to be investigated. Fouling of heat exchange surfaces with
proteinaceous foods still needs
development, as evidenced by a recent issue of the Transactions
of the Institution of Chemical Engineers devoted entirely to the
subject (Dun- and Grasshoff, 1999;
Gillham et al., 1999; Robbins et al., 1999).
B2. Microwave Heating Making food products microwaveable
is still one of the top aspirations in the U.S. food industry.
Another area of industrial importance is
the use of microwaves in processes such as sterilization for improved
quality. Heat and moisture transfer associated with microwave
heating of food can have a
major impact on the final quality of foods.
Collaborative work between PA and NY-Ithaca stations has led
to a comprehensive book on microwave processing of food (Datta
and Anantheswaran, 2000). It
is the most complete collection of information for the U.S. food
industry in developing innovative microwave food products and
processes. Collaboration between
OH and NY-Ithaca station has also been useful in developing a
Symposium on Microwave Food Sterilization during the IFT 2000
Annual Meeting.
Heating non-uniformity of microwaves due to product and equipment
variables are of great significance. Accurate models of heating
non-uniformity were developed
by coupling the electromagnetics and heat transfer and validating
the results using chemical marker formation. Only through such
coupling was it possible to
demonstrate how the cold point in a sterilization process changes
during the heating, with major implication to safety of such processes.
Enhanced heating (focusing)
in certain food shapes and properties, that lead to unusual (compared
with conventional) heating and moisture transport were identified
(Zhang and Datta, 1999).
These provide guidelines for all product and process development,
although application to differential heating of food components
in a multi-compartment frozen
dinner was studied in detail. Microwave pasteurization of shell
eggs without major protein denaturation was studied in the Illinois
station (Sullivan and Padua, 1999).
Understanding moisture transport in microwave heating should
lead to reduction of sogginess and over-drying of foods heated
in microwaves. Experimental moisture
profiles as affected by heating parameters were studied (Zhou
et al., 1995; Lin et al., 1995). Heat and mass transfer coefficients,
important for quantitative
understanding of heat and moisture transfer was measured (Mukherjee
et al., 1997). A comprehensive multiphase porous media transport
model (Ni et al., 1999)
identified the various modes of moisture transport, such as capillarity
and pressure driven ' flow. Pressure gradients in the microwaved
food due to internal heating
and vaporization significantly enhance the moisture transport
making the food surface soggy and increasing the moisture loss.
Infrared and hot air-assisted microwave heating of food to
reduce surface sogginess of microwaved foods was studied (Datta
and Ni, 1999). When absorbed
mostly on the surface, infrared can reduce surface moisture and,
beyond a threshold power level, it can reduce the' surface moisture
to lower than its initial value. Hot
air also can reduce surface moisture and increase surface temperature,
but not as effectively as infrared heat. These findings are important
for designing products and
processes for combination microwave/ infrared/ hot air heating
as they have begun to appear in domestic microwave ovens.
B3. Frying Reduction of oil pickup by fried foods while
achieving the right texture and flavor is of considerable interest
to the U.S. food industry and consumers. To
achieve this objective will require the understanding of heat
transfer, moisture evaporation, moisture movement in liquid and
vapor phase and oil pickup during frying.
Convective heat transfer coefficient measures the rate of heat
transfer from the oil to the food product and has a major influence
on all aspects of the frying process.
The rapid boiling at the surface of food makes this convective
heat transfer a complex process. The convective heat transfer
coefficient was measured (CA, NC,
OH, and TX Stations) using the lumped parameter approach. These
measurements permit a better understanding of the heat transfer
mechanism at the food surface
during frying.
The convective heat transfer coefficient decreases as the oil
degrades during frying and the coefficient increases with oil
temperature. Mass transfer during frying
consists of moisture loss and oil absorption. Moisture loss in
chips (tortilla chips) was found to decrease exponentially with
frying time. Oil absorption is a complex
phenomenon. Studies on tortilla chips at the TX station suggest
that most of the oil does not penetrate the product during frying,
but during the cooling period when
the product is removed from the fryer. Detailed experimentation
was developed to identify the relative amounts of oil pickup on
the surface and inside the food
material.
Future Needs: Work is still needed in better characterization
of energy, moisture and oil movements in the product during continuous
frying or batch frying. The
effects of water evaporation and the shrinkage of food matrix
on the oil absorption have not been understood.
B4. Extrusion Extrusion is an extremely useful but a
complex process to the food industry, involving heat transfer,
moisture transfer, rheology and kinetics. Studies
on extrusion of foods benefit development of new and value-added
products, including alternative non-food uses of agricultural
material. Constitutive models and
equations are being applied to analyze the rheo logical behavior
and flow patterns in extruders during extrusion of corn meal,
corn starches, and wheat starches at
MN, MO, NJ, and TX stations (Zhang and Bhattacharya, 1996; Tsue
- Er et al, 1998). In addition, MO and TX stations are also developing
adaptive control and
generalized predictive control (GPC) schemes for food extruders
(Tsue - Er et al., 1998; Xie, 1999). IL and MO stations are studying
the influence of raw material
characteristics, such as particle size and genetics on extrusion
processing efficiency (Garber et al., 1997; Faller et al., 1995).
Future needs: A more systematic approach to food extrusion
is needed so that the results are easier for scale-up and more
transferable from one model of extruder
to another model or from one screw configuration to another screw
configuration. Elucidation of changes in the rheo logical behavior
of dough in the extruder and at
the die region and their relationship with mechanisms of bubble
formation, extrudate expansion, and final extrudate texture were
studied. A robust, adaptive,
multi-input and multi-output, and easy-to-implement food extruder
controller needs to be developed. A better understanding of the
impact of raw material
characteristics on extrusion process efficiency is needed.
B5. Drying Superheated steam impingement drying is a
novel technology with potential for food applications. It has
advantages such as higher efficiency and
reduced oxidation, and was studied at the TX station. Under the
same conditions, superheated steam drying showed a shorter plateau
than air drying of corn tortillas.
The effect of temperature and airflow rate on the drying rate
and product quality attributes (porosity, shrinkage, texture,
degree of gelatinization) were studied.
Tortilla dries faster and becomes more porous at higher temperature
but shrinks more at low airflow rates. These studies will allow
optimization of this novel drying
process with potential to produce food products with better texture,
less quality loss, and increased speed of drying.
B6. Baking The important food process of baking had
not been understood quantitatively. Heat and mass transfer in
a slab of potato during baking were explained
using a multiphase porous media model (Ni and Datta, 1999). Baking
time reduces significantly with thickness, however at a slower
rate compared to
conduction-only heating. In addition, the surface temperature
also reaches a higher value for a thinner material, which may
help develop the often desired crusty
surface. The skin layer formed during baking can reduce the vapor
loss from the surface, and consequently increase the surface temperature
and center temperature
so that the baking time can be reduced. Decreasing initial moisture
content in the food and increasing air temperature and the heat
transfer coefficient reduces baking
time. This information would be valuable for the design and optimization
of industrial baking processes. Baking of tortillas is being investigated
at IN and TX stations.
B7. Modified Atmosphere Packaging (MAP) MAP for fresh
produce involves packaging with a gas-permeable polymeric film
to obtain a self-generated change
in the gaseous composition in the package. The exact composition
of the gas in the package is a dynamic function of the product
respiration rate and oxygen
transmission rate through the package and can be achieved by selecting
a polymeric film with the appropriate permeability and the amount
of produce in the
package. The optimum 0 2 concentration for mushrooms was found
to be 6% by the PA station (Roy et al., 1995a). They also noted
the need to maintain a constant
temperature (reduce temperature abuse) of the package to maintain
the desired gas concentration within the package. This could potentially
lead to food safety
concerns since a minimum of 5% 0 2 needs to be maintained within
the mushroom package to prevent the growth of anaerobic bacteria
such as C. botulinum.
Modified humidity packaging, which does not have the associated
risks of growth in C. botulinum with temperature abuse, can improve
the present shelf life of retail
mushrooms (Roy et al., 1995b). Suitability of newly developed
microperforated films was also studied (Ghosh, 1998). These findings
are paving ground for the
introduction of new packaging methods and films for the industry
to improve the shelf life of fresh mushrooms. IL station is investigating
the ability of corn proteins to
act as gas permeable polymeric film in MAP and storage of fresh
broccoli (Rakotonirainy, 1999). MAP technologies for MRE products
for the military were
developed by the NCFST and NJ stations, in collaboration with
industry and US Army Laboratories at Natick.
Future needs: Microperforated films can be effectively
used to develop a modified humidity package for fresh produce
to increase its shelf life. There is a need to
develop measurement techniques to monitor water vapor transmission
ratio (WVTR) of microperforated films, and to develop models to
predict WVTR as a
function of size and number of perforations.
B8. Use of Magnetic Resonance Imaging to Fluid Flow, Heat
Transfer and Mass Transfer The advantage of using magnetic
resonance imaging (MRI)
compared to traditional experimental methods is that MRI provides
spatially localized information as compared to an average over
the entire sample. Information is
also obtained non-invasively and hence does not disturb the process.
This permits new insight into the dynamics of heat, mass and momentum
transfer in foods during
processing, needed for product and process development. Significant
results using MRI to study thermal processing include: (1) the
measurement of velocity profiles
of non-Newtonian fluids in extruders; (2) simultaneous measurement
of velocity and concentration profiles in tube flow and in a scraped
surface heat exchanger; (3)
measurement of experimental data to develop a relationship between
flow behavior and strain history. Results are used to develop
new process control sensors that
maintain product quality and minimize production cost, and to
improve equipment design for promoting improved/uniform heat transfer.
OBJECTIVE C: To Develop Mathematical Models, Based on Objectives
A and/or B, For the Analysis, Design, and Improvement of Thermal
Processes.
Cl. Frying A mathematical model based on fundamental physical
principles will make the frying process more predictable as a
function of various operating
parameters. Such a model will help design better product, process
and equipment with less trial and error. This should lead to more
predictable final product quality,
improved process efficiency, reduced waste, more accurate control,
and microbiologically safer fried foods.
Mathematical models of frying, based on fundamental principles,
were developed by the California, NY-Ithaca, and TX stations.
Models developed at the CA and
NY-Ithaca stations apply to the frying of a single chip. California
station divided the material into wet and dry (crust) regions
and was able to predict temperatures,
moisture loss and crust development during frying. NY-Ithaca station
applied a more rigorous model by treating the food as a porous
media and considering
movement of heat, water, vapor and oil separately by the mechanisms
of diffusion, capillarity and pressure driven (Darcy) flow (Ni
and Datta, 1998). This showed
the relative importance of the three modes of transport in various
regions of the food during the frying process. A heat and mass
transfer model developed at the TX
station applied to a batch of tortilla chips and it predicted
oil temperature changes during such heating. Another observational
model predicted the dynamics of a
continuous fryer and was used to develop a controller for process.
Impact of this has been a quantum leap in the understanding of
the frying process that is used to
improve product quality, reduce oil pickup and optimize the process.
Computer-aided models of frying has been made available to the
industry for commercial
applications (CA).
Future Needs: Work in deep-fat frying is still under
way in many stations. Although great advances have been made in
the area of simulation and fundamental
understanding of deep-fat frying, models that can predict changes
in the product structure and volume as well as oil absorption
during frying and after frying are still
required. A fundamental physics-based model of a continuous frying
process is another area of critical need.
C2. Traditional Thermal Processing (Canning) Mathematical
models through the use of computer simulation were developed at
the Florida station for the
analysis, design, optimization and control of thermal processes
used in canned food sterilization. These models can be used to
predict the product temperature
history at any specified location within the can for any set of
processing conditions and container size; thus, precluding the
need to carry out repeated heat
penetration tests in the laboratory or pilot plant for alternate
process designs. A second advantage is that the retort temperature
need not be held constant, but can
vary in any prescribed manner.
An important application of these models is in the rapid evaluation
of an unscheduled process deviation, such as when an unexpected
drop in retort temperature
occurs during the process. The current practice in case of such
a deviation is to set aside whole batch of product (for batch
processing) to be judged safe by a
competent authority before releasing for shipment; otherwise the
complete batch of product must be reprocessed or destroyed. Such
practices are very costly and
inefficient and finding their alternatives is a critical need
for the canning industry. The models resulting from this project
are now being applied toward development of
intelligent on-line computer-based retort control systems capable
of rapid evaluation, on-line correction, and printed documentation
of any process deviations that
should occur while the process is still underway in real time.
This would allow for the release of all product batches on schedule
with full documentation in
compliance with government regulations (Teixeira et al., 1999).
These models have already been adopted for routine use by the
National Food Processors
Association (NFPA), and have been modified for application to
intelligent on-line process control by firms specializing in instrumentation
and control systems for the
food industry. The net impact of this work has been significant
cost reduction while assuring food safety at maximum quality.
In another study, a fundamental and comprehensive model showed
the development of broken heating during sterilization of canned
starch dispersions (Yang and
Rao, 1998b). This quantitative understanding of heating of starch
containing foods can have major impact in the improvement of thermal
processes for such foods.
C3. Microwave Sterilization Use of microwaves instead
of, or in combination with, conventional heating can produce sterilized
foods of much improved quality.
Significant advances were made in developing accurate and comprehensive
pictures of microwave food sterilization (Zhang and Datta, 1999).
Extensive numerical
modeling and experimentation using chemical marker formation to
verify models was performed. Unlike conventional sterilization,
heating patterns can change
qualitatively with geometry and properties (composition) of the
food material and an optimal heating is possible with their suitable
combinations. Combined with
chemical marker yield measurements, the numerical model can give
comprehensive descriptions of the spatial time- temperature history,
and thus be used to verify
and establish microwave sterilization processes.
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Swartzel, K.R. and Simunovic, J. 199X. Thermal Processor Measurement
Using Simulated Food Particles .PCT. The International Bureau
ofWIPO, Geneva,
Switzerland. In review.
Wu, S., Fratzke, A.R. and Murphy, P.A. 1998. A simple, low cost, high yield method for soybean glycinin and B-conglycinin separation. Patent applied.
Zhang, Q., B-L. Qin, G. V. Barbosa-Canovas, B. G. Swanson and
P. D. Pedrow. 1996. "Batch Mode Food Treatment Using Pulsed
Electric Fields." US Patent
No. 5,549,041
APPENDIX B
UNIQUE STATION CAPABILITIES AVAILABLE FOR
COLLABORATIVE PROJECTS
California
Dynamic Solid Analyzer.. Rheometrics
Differential Scanning Calorimeter .. Perkin Elmer
Video microscope 50X ... Olympus
Walk-in Freezer with wind tunnel
GC and HPLC ... HP and Waters
Florida
Fully-equipped semi-works citrus packing and processing pilot plant
State-of-the-art rotary retort, with full control capabilities
Closing machines for cans, glass, pouches, and semi-rigid containers
Facilities for research and testing of modified atmosphere packaging
Ultra-high pressure unit, 2.4 It capacity, -20 to 90C
Expertise in software development, especially in thermal processing
National high magnetic field lab
Food and Drug Administration
UV light reactor for juice processing.
Continuous unit is expected to be ready by FYOO. I
llinois (National Center for Food Safety and Technology)
Pilot scale Batch high pressure food processor
Pilot scale semi-continuous high pressure food processor
Laboratory scale pulsed electric field food processor
Equipment for determining thermal, physical & electrical properties of foods
Ozone processing system
NCFST is also in the process of installing a pilot scale aseptic processing system
Indiana
Aseptic packaging machine (Metal Box, single lane)
Supercritical Fluid Extractor (Isco)
Q-Test Texture Analyzer
Differential Scanning Calorimeter
NMR machines
Iowa
Linear Accelerator Facility - irradiation
High Pressure processing system
Soybean/soyfood commercial (Japanese system) processing pilot plant
Aroma/flavor/sensory testing equipment and human panelists (prob. similar to other stations Electronic Nose, GC, etc.)
Isoflavone analysis (samples sent here from all over the world)
Oil extraction from soybeans and oil seeds Haake and other rheological equipment
Michigan
Assessment of the interfacial behavior of biological macromolecules, particularly proteins
Acquiring and interpreting surface/interfacial tension data
Complete rheological analysis of fluid foods
Missouri
RheoStress RS100 (Haake, Paramus, NJ). A sophisticate rheometer
which allows rheological measurements under controlled stress
(CS), controlled rate (CR) and
oscillation (OSC) test modes.
Exstar 6100 Dynamic Mechanical Thermal analyzer (Seiko Instruments,
Chiba, Japan). This instrument has four modes of sample deformation
including
compression, tension, shear and bending, and is able to operate
from -150 to 600C at 0.01 to 20C/min heating and cooling rate
from 0.01 to lOOHz. It also has
Fourier transform technology in the noise reduction, and is able
to handle a wide range of materials from solid films to melts.
The Pyris 1 Differential Scanning Calorimetry with TAC 7/PC
Thermal Analysis Controller (Perkin-Elmer Corp., Norwalk, CT)
is a state-of-the-art computer
controlled laboratory instrument that operates with Perkin-Elmer's
unique power compensation design.
TA.XT2 Texture Analyzer with XTRA Dimension software (Texture
Technologies Corp., Scarsdale, NY). It provides force or distance
measurements in
compression or tension mode with a wide variety of available probes.
The Fox 200 heat flow meter instrument (LaserComp, Wakefield,
MA). A complete system with thermal conductivity instrument for
testing in accordance with
ASTM C518 and ISO 8301 specifications.
APV Baker 50/25 MPF intermeshing, co-rotating twin-screw extruder
(APV Baker, Grand Rapids, MI). This extruder is a pilot plant
model and is similar to but
more versatile than commercial extruders. Materials are conveyed
along an enclosed barrel where they are subjected to a combination
of heating, cooling, mixing
and shear. The screws can be built in any number of configurations
using five types of screw element. Maximum screw speed is 500
rev/min. The processing
chamber (barrel) has a length to diameter ratio (L/D) of 25:1
and splits along the horizontal axis for easy cleaning. The barrel
diameter is 50 mm. The barrel is heated
and cooled in zones. Each heating/cooling zone is 2.5 D long and
has an independent temperature controller giving heating or cooling
as required on a time
proportional basis. The feed port is provided with a detachable
feed chute and accepts feed from a K-tron twin-screw volumetric
feeder. A liquid feed port is
provided in each zone. These ports can also be used for measurement
of product temperature or pressure using industry standard probes.
The main drive power (28
kW) is provided by a silicon controlled rectifier, direct current
drive. The motor is coupled via a mechanical torque limit device
to a splitter/reduction gearbox to
drive the twin output shafts. A rigid box frame carries all the
components of the extruder.
Nebraska
C.W. Brabender Extruders - single and twin screw, mixing and non mixing configurations, and film blowing and compounding capabilities.
Permeability measurement of thin films - CO 2 and H:20
New Jersey
Laser Doppler Anemometer applications in extrusion
Jet impingement heat transfer applications to baking
Mechanical dynamic measurements of glass transition temperature
Intelligent microwave oven for more precise control of product residence time
FIDAP and FLUENT software for simulation of heat and mass transfer
Numerical simulation ofviscoelastic flows
New York (Geneva)
Isothermal Heating Apparatus (John Roberts).
This heating equipment incorporates a multi-mode microwave
oven with Variable continuous power and a feedback temperature
controller for rapid internal heating
along with variable convective hot air for rapid surface heating.
Utilizing these two heating mechanisms in a controlled system,
the operator is able to heat food
particulates below boiling temperatures isothermally and obtain
desired temperatures within seconds.
Temperature Data Acquisition in a Microwave Oven (John Roberts).
This data acquisition is an eight channel fiber-optic system that
is able to record
time-temperature measurements in a microwave environment. There
are many systems similar to this, but the uniqueness of this system
is that it is attached to the
rotating glass tray in a home microwave oven and the unit rotates
with the product on a slip-ring device. Thus temperature profiles
can be obtained in food products
as they heat and rotate in a home microwave oven.
AR 100 Rheometer, TA Instruments (Andy Rao) With this rheometer,
one can conduct flow, creep, and dynamic rheological tests, as
well as measure normal
stresses of fluid and semisolid foods. The Peltier temperature
control system can control the temperature of a test sample between
-20 to 180°C.
Dynamic Mechanical Analyzer (DMA), Model 2980, TA Instruments (Andy Rao)
The DMA should allow us to study the rheological properties of solid foods. We plan to use for studies on fruits and vegetables.
Fruit and Vegetable Processing Pilot Plant (Department ofFS&T)
The pilot plant is dedicated to processing of fruits and vegetables.
It is used to support food processors interested in production,
pasteurization, and concentration of
fruit juices, and canning of vegetables.
New-York (Ithaca)
Software, hardware and trained personnel for computational
modeling in heat transfer, mass transfer, thermo- and hygromechanics
and coupled
thermal-electromagnetics. Software includes commercial ones such
as FIDAP and FLUENT as well as home grown ones. The applications
in the past have been to
cracking during rapid freezing, electromagnetic field patterns
in microwave heating, and heat and moisture transfer in microwave
heating, infrared heating, baking and
frying.
Laboratory microwave oven with instrumentation to measure forward and reflected power and with mode stirrer to improve uniformity.
Fiberoptic temperature and pressure measurement system that is immune to electromagnetic interference, as in a microwave oven.
North Carolina
Continuous flow radio frequency unit 30 kW, 40.68 MHz
Manufacturer: Radio Frequency Co., Inc., Millis, MA
Applications: Uniform heating of viscous and particulate products
Software: CFD-ACE+ Vendor: CFD Research Corp., Huntsville,
AL; Applications: Modeling fluid flow, heat transfer (includes
grid generation and post-processing
also. Has capability to incorporate use defined subroutines)
Single and Multicoil heat exchangers Vendor: VRC Co., Cedar
Rapids, IA Applications: Rapid and uniform heating (ultrapasteurization)
; minimum to no fouling
Bohlin VOR controlled-strain rheometer
Haake VT-550 Viscotester
StressTech controlled stress rheometer with sealed cell attachment for couette geometry allows measurement of viscosity at temperatures higher than 100 °C
Electrorheological attachment for Haake VT550
MTS/histron Universal Testing machine
Differential Scanning Calorimeter, Perkin Elmer DSC 7 with modulated capability (Pyris 1) Dynamic Mechanical Analysis, Perkin Elmer
Micromeritics Helium Pycnometer: Determination of true and bulk particle density and porosity
International Paper SA-50 Aseptic Filler ( 250 ml aseptic brick
packs at 275 gal/hr with a minimum batch size of 100 gal; 3600
pkg/hr; single cycle: unfolded
pouches with a minimum batch size of 5 gal.)
Scholle 9-S auto-fill, extended life, bag-in-box filler; 1
- 3 gal; SchoUe Cheny Buirell EQ-3 ESL clean-fill filler (8, 16,
32 ounces; 26 - 70 units/min; half pint, quart
gable-top containers),
Cherry-Burrell, Cedar Rapids, IA.
North Dakota
Bench-scale solvent extraction
Mini expeller and other oilseed processing
Tofu/soy milk pilot plant
Ohio
PEF pilot facility with aseptic packaging
Ohmic heating pilot facility
High Pressure Processing facility
Continuous flow microwave processing units
Ozonation equipment
A high speed microscopic imaging system for imaging bacterial cells during PEF treatment.
Liquid crystal/image analysis temperature measurement
Particle tracking velocimetry capability for measurement of interstitial velocity and solids motion in multiphase flow.
PEF bacterial death kinetics equipment
Ohio Supercomputer Center, with various CFD and other computational codes.
Pennsylvania
Characterization of dielectric properties of food systems: Network analyzer, coaxial probe, transmission cell
Characterization of gas permeabilities of food packaging systems:
MOCON/Oxygen transmission rate measurement system, Permatran/Water vapor transmission rate measurement system
Continuously-variable-power microwave oven and fluoroptic temperature measurement system.
Texas
Snacks processing lab - tortilla chips processing
Rheological measurements lab (controlled stress rheometer, 2 Haakes, 3 Brookfields, 2 Texture Analyzers)
Vaccum and pressure frying units, permeability probe of porous media
Impingement drying (steam and air)
Extrusion (twin and single screw), reverse osmosis and ultrafiltration (membranes)
Washington
High Pressure Press
Wisconsin
Dynamic Mechanical Analysis (DMA): Perkin Elmer
Differential Scanning Calorimeter (DSC): Perkin Elmer DSC 7 and Perkin Elmer Pyris 1 with modulated capability
Submersible Microscope Probe: Lasentec PVM
Automated Image Analysis system: Nikon Labophot and Optiphot microscopes and Optimas 6.1 image analysis software
Refrigerated glove box (home made) for work on frozen foods
RELATED CURRENT AND PREVIOUS WORK
The following projects were identified through a search of the CRIS (U.S.) and ICAR (Canada) databases:
Projects involving NC-136 members:
Project Number: CA-D*-AER-3499-RR Performing Organization:
AGRI ENGINEERING Performing Institution: UNIV OF CALIFORNIA Investigator(s):
SINGH R P Project Title- IMPROVEMENT OF THERMAL PROCESSES FOR
FOODS.
Project Number: CA-D*-FST-5641-RR Performing Organization:
FOOD SCIENCE AND TECHNOLOGY Performing Institution: UNIV OF CALIFORNIA
Investigators)- MCCARTHY M J MCCARTHY K L Project Title: IMPROVEMENT
OF THERMAL PROCESSES FOR FOODS.
Project Number: FLA-AGE-03456 Performing Organization: AGRI
ENGINEERING Performing Institution: UNIVERSITY OF FLORIDA Investigators):
TEDCEIRA A A SMERAGE G H Project Title: IMPROVEMENT OF THERMAL
PROCESSES FOR FOODS.
Project Number: ILLW-NC-136 Performing Organization: NATIONAL
CNTR FOR FOOD SAFETY Performing Institution: ILLINOIS INSTITUTE
OF
TECHNOLOGY Investigators)- BALASUBRAMANIAM VM Project Title: IMPROVEMENT
OF THERMAL PROCESSING FOR FOODS.
Project Number: ILLR-9603758 Performing Organization: NATL
CENTER FOR FOOD SAFETY & Performing Institution: ILLINOIS
INSTITUTE OF
TECHNOLOGY Investigator(s): BALASUBRAMANIAM JM Project Title:
ELECTRICAL RESISTANCE HEATING OF MULTIPHASE FOODS.
Project Number: ILLU-69-0201 Performing Organization: UNIVERSITY
ADMINISTRATION Performing Institution: UNIVERSITY OF ILLINOIS
Investigator(s): BALASUBRAMANIAM V PALANIAPPAN S REDDY R Project
Title: HIGH ISOSTATIC PRESSURE INACTIVATION OF SELECTED
FOOD SPOILAGE MICRORGANISMS .
Project Number: IND060017A Performing Organization: FOOD SCIENCE
Performing Institution: PURDUE UNIVERSITY Investigator(s): MARKS
J S Project
Title- IMPROVEMENT OF THERMAL PROCESSES FOR FOODS.
Project Number: IOW02164 Performing Organization: FOOD TECHNOLOGY
Performing Institution: IOWA STATE UNIVERSITY Investigator(s):
WILSON
L A NIKOLOV Z L MURPHY P A Project Title: IMPROVEMENT OF THERMAL
PROCESSES FOR FOODS.
Project Number: MIN-12-030 Performing Organization: AGRI ENGINEERING
Performing Institution: UNIV OF MINNESOTA Investigator(s):
BHATTACHARYA M K APOOR B Project Title: IMPROVEMENT OF THERMAL
PROCESSES FOR FOODS.
Project Number: NC00836 Performing Organization: FOOD SCIENCE
Performing Institution: NORTH CAROLINA STATE UNIV Investigators):
FARKAS B
E SWARTZEL K R Project Title: IMPROVEMENT OF THERMAL PROCESSES
FOR FOODS .
Project Number: NC05483 Performing Organization: FOOD SCIENCE
Performing Institution: NORTH CAROLINA STATE UNIV Investigator(s):
DAUBERT
C R Project Title: RHEOLOGICAL PROPERTIES OF FOOD AND BIOLOGICAL
SYSTEMS.
Project Number: NC05859 Performing Organization: FOOD SCIENCE
Performing Institution: NORTH CAROLINA STATE UNIV Investigator(s):
SANDEEP
K P SWARTZEL K R Project Title: ENGINEERING STUDIES ON CONTINUOUS
FLOW THERMAL PROCESSES FOR FLUID FOODS .
Project Number: NC06393 Performing Organization: FOOD SCIENCE
Performing Institution: NORTH CAROLINA STATE UNIV Investigators):
FARKAS BE
Project Title: PHASE CHANGE AND MOVING BOUNDARY PROBLEMS IN FOOD
PROCESSING OPERATIONS.
Project Number: NC06482 Performing Organization: FOOD SCIENCE
Performing Institution: NORTH CAROLINA STATE UNIV Investigators):
KEENER
KM Project Title: TRANSPORT PHENOMENA IN AGRICULTURAL AND BIOLOGICAL
PROCESSES.
Project Number: ND01452 Performing Organization: AGRI ENGINEERING
Performing Institution: NORTH DAKOTA STATE UNIV Investigator(s):
WIESENBORN D P Project Title: IMPROVEMENT OF THERMAL PROCESSES
FOR FOODS.
Project Number: NEB-11-044 Performing Organization: BIOLOGICAL
SYSTEMS ENGINEERING Performing Institution: UNIVERSITY OF NEBRASKA
Investigator(s): HANNA M A CHINNASWAMY R Project Title: IMPROVEMENT
OF THERMAL PROCESSES FOR FOODS .
Project Number: NYG623493 Performing Organization: FOOD SCIENCE
AND TECHNOLOGY Performing Institution: N Y AGRICULTURE EXPT
STATION Investigator(s): RAO M A WALTER R H Project Title: IMPROVEMENT
OF THERMAL PROCESSES FOR FOODS.
Project Number: NYG623560 Performing Organization: FOOD SCIENCE
AND TECHNOLOGY Performing Institution: N Y AGRICULTURE EXPT
STATION Investigator(s): RAO MA WALKER LP Project Title: ROLE
OF GRANULE SIZE AND VISCOMETER GEOMETRY IN RHEQLOGY OF
STARCH DISPERSIONS.
Project Number: OH000768-SS Performing Organization: AGRI ENGINEERING
Performing Institution: OHIO STATE UNIV Investigator(s): SASTRY
S K
Project Title: OHMIC HEATING AND RAPID COOLING OF SOLID-LIQUID
MDCTURES.
Project Number: TEX03366 Performing Organization: AGRI ENGINEERING
Performing Institution: TEXAS A&M UNIV Investigator(s): MOREIRA
R G
LACEY R E SWEAT V E Project Title: IMPROVEMENT OF THERMAL PROCESSES
FOR FOODS.
Project Number: WNP00223 Performing Organization: BIOLOGICAL
SYSTEMS ENGINEERING Performing Institution: WASHINGTON STATE
UNIVERSITY Investigators): TANG J CAVALIERI R P PITTS M J Project
Title: APPLICATION OF MICROWAVE HEATING IN FOOD AND
AGRICULTURE PROCESSES . Other related U.S. Projects:
Project Number: 6612-41420-003-OOD Performing Institution:
AGRICULTURAL RESEARCH SERVICE Investigators): DICKENS J A CASON
JR J A
BUHR R J Project Title: ENGINEERING INNOVATIONS AND MICRO DEVELOPMENTS
TO REDUCE CONTAMINATIO N OF POULTRY AND
EQUIPMENT.
Project Number: 1935-41420-001-OOD Performing Organization:
AGRICULTURAL RESEARCH SERVICE Performing Institution: EASTERN
REGIONAL
RES CENTER Investigator(s): MORGAN A I GOLDBERG N M Project Title:
DESIGN OF PROTOTYPE SURFACE PASTEURIZER FOR FRESH MEATS
AND POULTRY.
Project Number: ARK01677 Performing Organization: BIOLOGICAL
& AGR ENGINEERING Performing Institution: UNIVERSITY OF ARKANSAS
Investigator(s): MARKS B P MARCY J A SIEBENMORGEN T J Project
Title: QUANTIFYING THE DEGREE OF COOKING FOR
FURTHER-PROCESSED POULTRY PRODUCTS.
Project Number: CA-D*-FST-6462-H Performing Organization: FOOD
SCIENCE AND TECHNOLOGY Performing Institution: UNIV OF CALIFORNIA
Investigators): SHOEMAKERCF Project Title: THE EFFECT OF FOOD
POLYMER COMPOSITION AND STRUCTURE ON THE RHEOLOGY AND
TEXTURE OFFOODS .
Project Number: GE001500 Performing Organization: FOOD SCIENCE
AND TECHNOLOGY Performing Institution: UNIVERSITY OF GEORGIA
Investigator(s): HUNG Y C Project Title- VALUE-ADDED PROCESSES
TO ENHANCE THE QUALITY AND SAFETY OF FOODS.
Project Number: IND046058 Performing Organization: AGRI ENGINEERING
Performing Institution: PURDUE UNIVERSITY Investigator(s): HAGHIGHI
K
Project Title- APPLICATION OF FINITE ELEMENT TO PRODUCTION AND
PROCESSING OF FOOD AGR. AND BIOLOGICAL MATERIALS .
Project Number: MAS-9502429 Performing Organization: FOOD SCIENCE
Performing Institution: UNIV OF MASSACHUSETTS Investigator(s):
PELEG M
Project Title- IMPERFECT SQUEEZING FLOW VISCOSIMETRY FOR FOOD
PRODUCTS.
: MAS09701494 Performing Organization: FOOD SCIENCE Performing
Institution: UNIV OF MASSACHUSETTS Investigator(s): MCCLEMENTS
D J
Project Title- NON-DESTRUCTIVE CHARACTERIZATION OF FOOD EMULSIONS
USING ULTRASOUND.
Project Number: NYG623559 Performing Organization: FOOD SCIENCE
AND TECHNOLOGY Performing Institution: N Y AGRICULTURE EXPT
STATION Investigator(s): SPLITTSTOESSER D P MCLELLAN M R Project
Title: PASTEURIZATION PROCESSES FOR THE DESTRUCTION OF
ESCHERICHIA COLI 0157:H7 IN SWEET CIDER. P
Project Number: TEN00125 Performing Organization: FOOD SCIENCE
AND TECHNOLOGY Performing Institution: UNIVERSITY OF TENNESSEE
Investigator(s): HULBERT G J RAMAN R WILHELM L Project Title:
ENGINEERING SYSTEMS FOR VALUE-ADDED FOOD PROCESSING AND
WASTE UTILIZATION.
Project Number: UTA00226 Performing Organization: NUTRITION
& FOOD SCIENCE Performing Institution: UTAH STATE UNIVERSITY
Investigator(s):
MCMAHON D IRUDAYARAJ J Project Title: EVALUATION OF ELECTROHEATING
TECHNOLOGY FOR UHT PROCESSING OF MILK.
Project Number: VA-135503 Performing Organization: FOOD SCIENCE
AND TECHNOLOGY Performing Institution: VIRGINIA POLYTECHNIC
INSTITUTE Investigators): PffiRSON M D Project Title: DESTRUCTION
OF CLOSTRIDIUM BOTULINUM IN FOODS AT MINIMAL PROCESSING
TEMPERATURES .
Project Number: 5325-42000-024-OOD Performing Institution:
WESTERN REGIONAL RES CENTER Investigators): TSAI L S HERNLEM B
J
ROBERTSON G H Project Title: ADV. TECHNOLOGIES FOR REDUCTION OF
MICROORGANISMS AND PARTICULATE MATTER IN FOOD
PROCESSING .
Project Number: WIS04015 Performing Organization: BIOLOGICAL
SYSTEMS ENGINEERING Performing Institution: UNIV OF WISCONSIN
Investigator(s): GUNASEKARAN S Project Title: RHEOLOGICAL PROPERTIES
OF BIOPOLYMER GEL SYSTEMS.
Related Canadian Research Projects
Project Number: 333-1411-9611 AGRICULTURE AND AGRI-FOOD CANADA
RESEARCH BRANCH FOOD RESEARCH AND DEVELOPMENT
CENTREPASSEY C A Development of separation and fractionation technologies
for value-added processing of milkfat.
Project Number: 11680 Performing Organization: UNIVERSITY OF
GUELPH, COLLEGE OF PHYSICAL AND ENGINEERING SCIENCES Investigator(s):
BROWN R TECH Project Title: Digital image analysis and interpretation
in food processing and grading systems.
Project Number: 11270 Performing Organization: UNIVERSITY OF
GUELPH, ONTARIO AGRICULTURAL COLLEGE Investigators): TUNG M TECH
Project Title: Temperature controlled food packaging for improved
shelf life, quality and safety.
Project Number: 16430 Performing Organization: UNIVERSITY OF
GUELPH, ONTARIO AGRICULTURAL COLLEGE Investigators): MCKNIGHT
D
TECH Project Title: Sanitizing milk lines and milk handling equipment
with special references to rubber hoses, gaskets and inflations.
Project Number: AGENG022 UNIVERSITY OF MANITOBA FACULTY OF
AGRICULTURAL AND FOOD SCIENCES JAYAS D S Optimization of
canned food sterilization and measurement of thermal properties
of irregular shaped food materials.
Project Number: 11430 Performing Organization: UNIVERSITY OF
GUELPH COLLEGE OF PHYSICAL AND ENGINEERING SCIENCES Investigators).
MITTAL G TECH Project Title: To investigate the mechanisms of
food frying processes for lower fat and better quality products.
Performing Organization:
MACDONALD CAMPUS OF MCGILL UNIVERSITY FACULTY OF AGRICULTURAL
AND ENVIRONMENTAL SCIENCES Performing Institution:
21-111 Lakeshore Road Investigators): RAMASWAMY H SABLANI S Project
Title: Quality enhancement of foods through rotational processing.
Performing
Organization: MACDONALD CAMPUS OF MCGILL UNIVERSITY FACULTY OF
AGRICULTURAL AND ENVIRONMENTAL SCIENCES Performing
Institution: 21-111 Lakeshore Road Investigators): RAMASWAMY H
GRABOWSKI S TAJCHAVAVIT S Project Title: Heat transfer techniques
for improved
food processing.
Project Number: 333-1421-9307 Performing Organization: AGRICULTURE
AND AGRI- FOOD CANADA RESEARCH BRANCH FOOD RESEARCH
AND DEVELOPMENT CENTRE Performing Institution: 3600 Casavant Boulevard
West Investigator(s): MARCOTTE M Project Title: Amelioration de
la qualite
des aliments par Ie developpement ou la mise au point de traitements
thermiques de stabilisation. 107